| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 5277615 | Tetrahedron Letters | 2008 | 4 Pages |
Abstract
A wide range of commercial diazodicarboxylates and phosphines were screened in an attempt to find purification-free conditions for application in parallel synthesis. The combination of immobilized triphenylphosphine and TMAD proved to be suitable for the synthesis of aryl ethers via the Mitsunobu reaction. Nine ethers were synthesized in good yield and excellent purity, the purification being limited to a filtration step.
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Related Topics
Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Eric Valeur, Didier Roche,