| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 5284347 | Tetrahedron Letters | 2008 | 4 Pages |
Suzuki-Miyaura reactions using Pd/PVP as a catalyst source were carried out in water-ethanol solution. Under MW, sonication or thermal condition yields were very similar, from moderate to very good, in a variety of examples. However, TOFs were very different, 750/h under MW, 250/h under sonication, and 28/h under thermal conditions. Studies carried out under sonication showed that the whole system after product extraction can be re-used at least twice without any noticeable loss of yield.
Graphical abstractSuzuki-Miyaura reactions using Pd/PVP as a catalyst source were carried out in water-ethanol solution. Yields (and TONs) were very similar under any of the conditions studied. However, TOFs were very differents, 750/h under MW, 250/h under sonication and 28/h under thermal conditions. Studies carried out under sonication showed that the whole system after product extraction can be re-used at least twice without any noticeable loss of yield.Download full-size image
