Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5284672 | Tetrahedron Letters | 2008 | 4 Pages |
Abstract
Red phosphorus reacts with 1-(tert-butyl)-4-vinylbenzene in a superbase media (KOH-DMSO, 90-100 °C, 3 h) to give tris[4-(tert-butyl)phenethyl]phosphine oxide in 77% yield. Microwave activation of the reaction affords the phosphine oxide in 82% yield in 6 min.
Related Topics
Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Boris A. Trofimov, Svetlana F. Malysheva, Nina K. Gusarova, Vladimir A. Kuimov, Nataliya A. Belogorlova, Boris G. Sukhov,