Article ID Journal Published Year Pages File Type
5284672 Tetrahedron Letters 2008 4 Pages PDF
Abstract
Red phosphorus reacts with 1-(tert-butyl)-4-vinylbenzene in a superbase media (KOH-DMSO, 90-100 °C, 3 h) to give tris[4-(tert-butyl)phenethyl]phosphine oxide in 77% yield. Microwave activation of the reaction affords the phosphine oxide in 82% yield in 6 min.
Related Topics
Physical Sciences and Engineering Chemistry Organic Chemistry
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