Article ID Journal Published Year Pages File Type
5285367 Tetrahedron Letters 2006 6 Pages PDF
Abstract
The stereospecific synthesis of the dienophile subunit precursor D was achieved from the butenolide E. The ester corresponding to the precursor of A was obtained in 67% overall yield from the aldehyde C, via a chlorite oxidation and subsequent Mitsunobu reaction of the acid B with D. Tentative IMDA reactions of A did not presently afford the adduct (thermal or Lewis acid catalysis conditions).
Related Topics
Physical Sciences and Engineering Chemistry Organic Chemistry
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