| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 5405541 | Journal of Magnetic Resonance | 2013 | 7 Pages |
Abstract
- Effect of low-temperature MAS experiments on a membrane protein is investigated.
- Sensitivity is significantly enhanced but the resolution is decreased at 100Â K.
- Variation of spin-lattice relaxation (T1) with temperature is reported.
- T1 values are significantly reduced using a small amount of Cu2+-chelated lipid.
- 2D RFDR spectrum of a uniformly 13C & 15N-labeled cytochrome-b5 is presented.
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Authors
Kazutoshi Yamamoto, Marc A. Caporini, Sangchoul Im, Lucy Waskell, Ayyalusamy Ramamoorthy,