Article ID Journal Published Year Pages File Type
5405863 Journal of Magnetic Resonance 2013 7 Pages PDF
Abstract
► Probe for solid state NMR with dynamic nuclear polarization (DNP) and magic-angle spinning (MAS) at 20 K and 9.4 Tesla. ► Signal enhancement greater than 25-fold (microwaves on versus microwaves off) using 30 mW of microwaves. ► 2D 13C-13C spectra for 160 nmol of the 26 residue peptide melittin in frozen solution, taken in ∼2½ h.
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Physical Sciences and Engineering Chemistry Physical and Theoretical Chemistry
Preview
Solid state nuclear magnetic resonance with magic-angle spinning and dynamic nuclear polarization below 25 K
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