Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5405979 | Journal of Magnetic Resonance | 2012 | 9 Pages |
Abstract
⺠DEER with very rapid freezing yielded broader distributions than regular freezing. ⺠Neither method of freezing altered the distance maxima. ⺠Rapid freezing yielded more uniform distribution of spin-labels and enhanced DEER S/N. ⺠Rapid frozen samples require less cryoprotectant than regularly frozen samples. ⺠Bromo-substituted spin-label produced narrower distance distributions..
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Physical Sciences and Engineering
Chemistry
Physical and Theoretical Chemistry
Authors
Elka R. Georgieva, Aritro S. Roy, Vladimir M. Grigoryants, Petr P. Borbat, Keith A. Earle, Charles P. Scholes, Jack H. Freed,