Article ID Journal Published Year Pages File Type
5406440 Journal of Magnetic Resonance 2011 7 Pages PDF
Abstract
► 13CH3, 13CH2D and 13CHD2 methyls are observed in spectra of partially deuterated proteins. ► In many NMR applications, 13CHD2 isotopomers are targeted because of their AX-like character. ► Simple pulse-scheme elements are presented for 'clean' detection of 13CHD2 isotopomers.
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Physical Sciences and Engineering Chemistry Physical and Theoretical Chemistry
Preview
Selective detection of 13CHD2 signals from a mixture of 13CH3/13CH2D/13CHD2 methyl isotopomers in proteins
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