Article ID Journal Published Year Pages File Type
5406459 Journal of Magnetic Resonance 2010 10 Pages PDF
Abstract
► The effect of the proton offset in 15N-{1H} NOE experiments is investigated. ► Various proton irradiation schemes are compared under normal and extreme conditions. ► Radiation damping may lead to inaccurate intensities in the reference experiment. ► A recipe to record 15N-{1H} NOE's is presented.
Keywords
Related Topics
Physical Sciences and Engineering Chemistry Physical and Theoretical Chemistry
Preview
On the measurement of 15N-{1H} nuclear Overhauser effects. 2. Effects of the saturation scheme and water signal suppression
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