Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5406853 | Journal of Magnetic Resonance | 2009 | 4 Pages |
Abstract
Two-dimensional 1H homonuclear correlation NMR spectra of solids of biological interest have been recorded at high magnetic fields (14.1 and 18.8 T) and MAS rates up to 67 kHz, using RNnν symmetry-based homonuclear recoupling and CRAMPS decoupling; this method affords exceptional spectral resolution and is well suited to probe 1H-1H proximities in powdered solids.
Related Topics
Physical Sciences and Engineering
Chemistry
Physical and Theoretical Chemistry
Authors
Luis Mafra, Renée Siegel, Christian Fernandez, Denis Schneider, Fabien Aussenac, João Rocha,