Article ID Journal Published Year Pages File Type
5407476 Journal of Magnetic Resonance 2007 8 Pages PDF
Abstract
The application of a spin-state-selective coherence transfer experiment (INADEQUATE-SSS) to solid-state NMR spectroscopy is described. Two-dimensional 13C double-quantum/single-quantum spectra without J splittings in both dimensions lead to enhanced spectral resolution. The method is demonstrated to significantly improve the spectral resolution of the crowded C′-Cα region of two proteins.
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Related Topics
Physical Sciences and Engineering Chemistry Physical and Theoretical Chemistry
Preview
Improved resolution in 13C solid-state spectra through spin-state-selection
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