Article ID Journal Published Year Pages File Type
5420576 Solid State Nuclear Magnetic Resonance 2011 6 Pages PDF
Abstract
► We collected 63Cu and 23Na MAS NMR spectra to 926 K on CuBr, CuI, and NaNbO3. ► Easily observed phase transitions serve as useful temperature calibration points. ► Large temperature effects on 63Cu shifts can also be useful for such calibrations.
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Physical Sciences and Engineering Chemistry Physical and Theoretical Chemistry
Preview
Temperature calibration for high-temperature MAS NMR to 913 K: 63Cu MAS NMR of CuBr and CuI, and 23Na MAS NMR of NaNbO3
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