Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5420605 | Solid State Nuclear Magnetic Resonance | 2011 | 7 Pages |
Abstract
⺠Simulation and experimental investigation of 1H resolution in 2D CRAMPS spectra. ⺠Effect of z-rotation and delays interleaved with the decoupling shape on 1H spectra during the indirect dimension. ⺠The best experimental 1H spectra along F1 dimension was obtained combining a z-rotation symmetry with delays. ⺠The best simulated 1H resolution achieved using the z-rotation without delays. ⺠Glycine and tyrosine·HCl amino acids used to test 2D 1H CRAMPS decoupling modifications during the indirect dimension.
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Authors
Renée Siegel, LuÃs Mafra, João Rocha,