Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5420861 | Solid State Nuclear Magnetic Resonance | 2009 | 6 Pages |
Abstract
We present two one-dimensional methods that allow direct observation of highly resolved 1H spectra in solid-state NMR. The methods, which work mainly at 30-35Â kHz MAS speeds, are very robust and efficient. In addition, they present very few false resonances. The windowed smooth amplitude-modulated (wSAM) version has a potential to work at ultra-fast MAS provided the electronics is capable to define the pulse-shape in a smooth way, without any pulse transients.
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Physical Sciences and Engineering
Chemistry
Physical and Theoretical Chemistry
Authors
Jean-Paul Amoureux, Bingwen Hu, Julien Trébosc, Qiang Wang, Olivier Lafon, Feng Deng,