Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5433138 | Dental Materials | 2016 | 11 Pages |
â¢Bond strength of composite cements to dentin was evaluated both by iFT and μTBS.â¢Î¼TBS appeared more discriminative than iFT for bonding effectiveness of cements to dentin.â¢Correlation between iFT and μTBS was moderate and not significant.â¢The etch-and-rinse and 'universal' self-etch composite cements performed best in both tests.
ObjectivesTo determine the interfacial fracture toughness (iFT) and micro-tensile strength (μTBS) of composite cements bonded to dentin.MethodsFifty feldspar ceramic blocks (Vita Mark II, Vita Zahnfabrik) were luted onto dentin using two self-adhesive (G-CEM LinkAce, GC; SpeedCEM, Ivoclar Vivadent), two self-etch (Multilink Primer & Multilink Automix, Ivoclar Vivadent; Scotchbond Universal & RelyX Ultimate, 3âM ESPE), and one etch-and-rinse (Excite F DSC & Variolink II, Ivoclar Vivadent) composite cement (n = 10). After 48 h in 100% relative humidity at 37 °C, one half of each tooth was sectioned in sticks with a chevron notch at the cement-dentin interface and tested in a 4-point bending test setup (iFT). The remaining half of the tooth was sectioned in micro-specimens and stressed in tension until failure (μTBS). The mode of failure was determined with a stereomicroscope at 50à magnification. Data were submitted to Weibull analysis and Pearson's correlation (α = 0.05).ResultsAt 10% probability of failure, no significant differences could be found using iFT, while the etch-and-rinse composite cement Variolink II presented a significantly higher μTBS at this level. At 63.2% probability of failure, the self-adhesive composite cement G-CEM LinkAce revealed a significantly lower μTBS and iFT, and the self-etch cement Multilink Automix also revealed a significantly lower μTBS than all other cements. The correlation found between iFT and μTBS was moderate and not significant (r2 = 0.618, p = 0.11).SignificanceOverall, the etch-and-rinse and 'universal' self-etch composite cements performed best. The micro-tensile bond strength and interfacial fracture toughness tests did not correlate well.
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