Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5439186 | Ceramics International | 2017 | 5 Pages |
Abstract
CaO doped nanofibrous zirconia (ZrO2) was fabricated by calcination of electrospun zirconium oxychloride (ZrOCl2)/ calcium nitrate (Ca(NO3)2)/polyethylene oxide (PEO) composite fibers. ZrO2 nanofibers were characterized by scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS) and X-ray diffractometry (XRD). It is revealed that CaO content variation in ceramic filaments calcined at 1200 °C allows fabricating fully monoclinic, or fully cubic zirconia nanofibers, or nanofibers containing both tetragonal and cubic phases. CaO stabilized fully tetragonal zirconia nanofibers can be prepared at lower calcination temperature.
Keywords
Related Topics
Physical Sciences and Engineering
Materials Science
Ceramics and Composites
Authors
Vyacheslav V. Rodaev, Andrey O. Zhigachev, Yuri I. Golovin,