Article ID Journal Published Year Pages File Type
5439964 Corrosion Science 2017 6 Pages PDF
Abstract

•Strain, defects and crystal orientation relationship in the initial oxidation stage of zirconium alloy were investigated.•An In-situ oxidation test and a short time exposure corrosion test were carried out.•Compressive strain between semi-coherent planes of m, t and c-ZrO2 was detected in a range from 0.3% to 6%.•Tensile strain in c-ZrO2 was detected in a range from 0 to 1.34%.

An In-situ oxidation test and a short time exposure corrosion test of Zircaloy-4 were carried out. A lot of dislocations generated in the nucleation and growth process of ZrO2 are observed. Dislocations will be firstly distributed at the interface of ZrO2. With the growth of m-ZrO2 grains, the number of dislocations at the interface increases. When the grain size of ZrO2 reaches a critical value, the dislocations in the grains of ZrO2 begin to appear. A compressive strain between semi-coherent planes of oxides was detected in a range from −0.3% to −6%.

Related Topics
Physical Sciences and Engineering Materials Science Ceramics and Composites
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