Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
5447534 | Journal of Physics and Chemistry of Solids | 2017 | 11 Pages |
Abstract
Monodispersed Fe-Co nanoparticles are synthesized by reducing FeCl2 and CoCl2 in diphenyl ether, with n-butyllithium as reducing agent and oleic acid as surfactant. The body centered cubic (BCC) crystal structure of Fe-Co nanoparticles is confirmed by both XRD patterns and TEM diffraction patterns. The average nanoparticle size is 10Â nm at the reported experimental condition. The magnetization of the Fe-Co increases with increased cobalt atomic percentage. XPS technique is used to investigate the surface chemical states of Fe-Co nanoparticles. Finally, the composition of Fe-Co nanoparticles is investigated through EDX, confirming the molar ratio of Fe/Co in nanoparticles could be accurately controlled by changing the composition of the precursors.
Keywords
Related Topics
Physical Sciences and Engineering
Materials Science
Electronic, Optical and Magnetic Materials
Authors
Yufeng Wang, Yi Zheng, Shuchun Hu,