Article ID Journal Published Year Pages File Type
582531 Journal of Hazardous Materials 2009 8 Pages PDF
Abstract
In the paper, the results of research the purity of DADNE in different recrystallization conditions and some intermediate products of its synthesis were presented. High performance liquid chromatography (HPLC) method based on the porous graphitic carbon (PGC) column packing material has been developed. Two variants of mobile phases in different pH values: acetonitrile-water and methanol-water with ammonia (NH3) and with trifluoroacetic acid (TFA) were used. The probable mechanism of interaction between the analyte, the stationary phase, and the mobile phase was suggested.
Related Topics
Physical Sciences and Engineering Chemical Engineering Chemical Health and Safety
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