Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
68732 | Journal of Molecular Catalysis A: Chemical | 2006 | 4 Pages |
A novel MCM-41-supported sulfur palladium(0) complex was conveniently prepared from commercially available and cheap γ-mercaptopropyltriethoxysilane via immobilization on MCM-41, followed by reacting with palladium chloride and then the reduction with hydrazine hydrate. This complex exhibited excellent performance in Sonogashira coupling reaction.
Graphical abstractA novel MCM-41-supported sulfur palladium(0) complex was conveniently prepared from commercially available and cheap γ-mercaptopropyltriethoxysilane via immobilization on MCM-41, followed by reacting with palladium chloride and then the reduction with hydrazine hydrate. This complex exhibited excellent performance in Sonogashira coupling reaction and can be reused without noticeable loss of activity. Figure optionsDownload full-size imageDownload as PowerPoint slide