Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7088428 | Chemical Engineering and Processing: Process Intensification | 2018 | 52 Pages |
Abstract
This study evaluated a new process for separation of aromatic compounds based on falling film distillation at thermosyphon-assisted atmospheric pressure (Destubcal Technology), in order to obtain enriched mass fractions of toluene in the distillate stream. Two compact experimental units were used: single-tube and multi-tubes on a pilot scale. The experimental tests were divided into two groups: isothermal and non-isothermal condition. The optimal feed mass flow rate, evaporator temperature and feed temperature conditions were found to be 25.13â¯kgâ¯hâ1, 102.10â¯Â°C and 132.90â¯Â°C, respectively, starting from a feed concentration of 43% (m/m). The best result was found by using the single-tube unit with about 25.24% (m/m) enrichment of mass fraction of toluene in the distillate stream. There was no relevant difference in results between the isothermal and non-isothermal conditions. The results found in the single-tube and multi-tubes pilot scale units were similar, showing toluene mass flow values at the distillate stream of 2.96â¯kgâ¯hâ1 and 44.76â¯kgâ¯hâ1 respectively; thus, they indicate high productivity. The new alternative for distillation of aromatic compounds proposed in this article shows a satisfactory result when compared to conventional distillation, because the Destubcal Technology had a lower energetic requirement.
Related Topics
Physical Sciences and Engineering
Chemical Engineering
Process Chemistry and Technology
Authors
Valdemar Francisco da Silva Filho, José Luiz Francisco Alves, Gabriel Francisco Reus, Ricardo Antonio Francisco Machado, Cintia Marangoni, Ariovaldo Bolzan,