| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 7589217 | Food Chemistry | 2016 | 7 Pages |
Abstract
Eleven oligosaccharides were isolated from sugar beet molasses using carbon-Celite column chromatography and HPLC. The constituent sugars and linkage positions were determined using methylation analysis, MALDI-TOF-MS, and NMR measurements. The configurations of isolated oligosaccharides were confirmed based on detailed NMR analysis. Based on our results, three of the 11 oligosaccharides were novel.
Keywords
MALDI–TOF-MSH2BCHPAECTOCSYSPTHSQCnuclear magnetic resonanceGC–FIDGC–MSOligosaccharideNMRgas chromatography–mass spectrometryTotal correlation spectroscopycorrelation spectroscopyHigh-performance anion-exchange chromatographyBeet molassesHMBC یا Heteronuclear Multiple Bond Correlationheteronuclear multiple bond correlationCOSYhigh-performance liquid chromatographyHPLCheteronuclear single quantum coherence
Related Topics
Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
Tatsuya Abe, Hiroto Kikuchi, Tsutomu Aritsuka, Yusuke Takata, Eri Fukushi, Yukiharu Fukushi, Jun Kawabata, Keiji Ueno, Shuichi Onodera, Norio Shiomi,