Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7599504 | Food Chemistry | 2014 | 7 Pages |
Abstract
Validation included investigation of linearity, selectivity, stability, limits of detection and quantitation, decision limit, detection capability, trueness, precision and ruggedness according to the Youden's approach. Limits of quantitation of examined tetracyclines were from 14.5 to 56.6 μg/kg significantly lower than respective Maximum Residue Limits, whereas recoveries ranged from 82.0% to 108%. The applicability of the method was evaluated using milk samples purchased from local market. Accuracy of the method was additionally proved by analysis of bovine milk certified reference material (BCR®-492).
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Authors
Eftichia Karageorgou, Marina Armeni, Ioulia Moschou, Victoria Samanidou,