Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7611762 | Journal of Chromatography A | 2015 | 7 Pages |
Abstract
The dynamic ranges of the calibration graphs and limits of detection are, respectively: 65-900 ng mLâ1 and 35 ng mLâ1 for marbofloxacin, 7.2-900 ng mLâ1 and 2.5 ng mLâ1 for ciprofloxacin, 6-900 ng mLâ1 and 2 ng mLâ1 for danofloxacin, 50-900 ng mLâ1 and 20 ng mLâ1 for enrofloxacin, 35-900 ng mLâ1 and 12 ng mLâ1 for sarafloxacin, 5-900 ng mLâ1 and 2 ng mLâ1 for oxolinic acid, and 7-900 ng mLâ1 and 2.5 ng mLâ1 for flumequine. The precision, established at two concentration levels of each analyte and expressed as the percentage of the relative standard deviation is in the range of 1.9-8.1% using standards, and of 3.4-10.7% in the presence of milk samples. The method has been satisfactorily applied to the analysis of skimmed, semi-skimmed and whole milk samples, with recoveries ranging from 89.0 to 106.5%.
Related Topics
Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
G.S. Yánez-Jácome, M.P. Aguilar-Caballos, A. Gómez-Hens,