Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7614326 | Journal of Chromatography A | 2013 | 9 Pages |
Abstract
⺠A UHPLC-MS/MS method is proposed for determination of 15 mycotoxins in milk thistle. ⺠Sample treatment is based on QuEChERS extraction and DLLME clean-up. ⺠LOQs are below maximum limits allowed by EU in foods and botanicals. ⺠RSDs were <10% and recoveries were >60%, except for ZON in seed and CIT in extract. ⺠The method could be good alternative for multi-mycotoxin determination in botanicals.
Related Topics
Physical Sciences and Engineering
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Analytical Chemistry
Authors
Natalia Arroyo-Manzanares, Ana M. GarcÃa-Campaña, Laura Gámiz-Gracia,