Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7614540 | Journal of Chromatography A | 2012 | 11 Pages |
Abstract
⺠Both methods are relevant for the purification of endogenous steroids in urine samples. ⺠For screening purpose, a one step MISPE protocol was developed followed by GC-MS analysis. ⺠For confirmatory purpose, SFC-MIP protocol gave sufficient purification before IRMS analysis. ⺠Developed methods are multiresidue and shorter and cheaper than published procedure. ⺠Testosterone, estradiol, nandrolone, and boldione abuse in bovine can be controlled.
Keywords
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Physical Sciences and Engineering
Chemistry
Analytical Chemistry
Authors
Mickael Doué, Emmanuelle Bichon, Gaud Dervilly-Pinel, Valérie Pichon, Florence Chapuis-Hugon, Eric Lesellier, Caroline West, Fabrice Monteau, Bruno Le Bizec,