Article ID Journal Published Year Pages File Type
7682728 Talanta 2013 6 Pages PDF
Abstract
The properties of silica modified with polyaniline such as particle size, porosity, average quantity of polyaniline covering carrier and density of sorbent were determined. In our study the following methods were used: microscopic analysis, laser diffraction technique, combustion analysis, mercury porosimetry and helium pycnometry. Column with the newly obtained packing was used for the separation of inorganic anions. Optimized chromatographic system was successfully employed for analysis of iodide and bromide in selected pharmaceutical products (Bochnia salt and Iwonicz salt) applied in chronic respiratory disease. Analysis was carried out using 0.1 M solution of HCl in mixture of methanol/water (50:50 v/v) as a mobile phase; the flow rate was 0.3 mL min−1, temperature was 24 °C and λ=210 nm. Validation parameters such as correlation coefficient, RSD values, recovery, detection and quantification limits were found to be satisfactory.
Related Topics
Physical Sciences and Engineering Chemistry Analytical Chemistry
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