Article ID Journal Published Year Pages File Type
7687732 TrAC Trends in Analytical Chemistry 2018 45 Pages PDF
Abstract
Participants were requested to analyse test solutions and extracts of various matrices with their method of choice. Thirty-three laboratories participated (9-22 per round), of which 55-81% were able to submit data. Large differences in results between laboratories were found (CVs 23-137%) but results improved over time, while the levels in the test materials decreased. In the last round acceptable CV values (<25%) were obtained for the test solution. In the last round, results obtained by the GC-ECNI-LRMS technique varied most, which is disconcerting as this technique is most commonly applied. We strongly suggest to continue monitoring comparability of laboratories to assess consensus in SCCP analysis, with a focus on quantification procedures applied.
Related Topics
Physical Sciences and Engineering Chemistry Analytical Chemistry
Authors
, , , ,