Article ID Journal Published Year Pages File Type
7889207 Ceramics International 2018 6 Pages PDF
Abstract
Al2O3 coatings with large specific surface were prepared on cast nickel-based superalloy K418 by cathode plasma electrolytic deposition (CPED) in aqueous solutions at different concentrations. The significance of energy consumption and a simple calculation method during CPED were proposed, and the influence of electrolyte concentration on current density-voltage curve, energy consumption, and microstructure of coatings were studied. It was found that increasing the concentration of electrolyte can effectively reduce the current density at the initial stage while prolonging the deposition time and stepping up the energy consumption of whole coating preparation. The morphology observation results showed that the pore size of Al2O3 coatings enlarges with the increase of the concentration, and the optimum electrolyte concentration is 0.5-1 mol L−1. Under this condition, the new method of oxidation pretreatment at 950 ℃ on samples for 30 min can efficiently decrease the current density during the early stage of preparation, which is beneficial to the deposition of complex-shaped samples with large size.
Related Topics
Physical Sciences and Engineering Materials Science Ceramics and Composites
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