Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7993588 | Journal of Alloys and Compounds | 2018 | 6 Pages |
Abstract
In this study, Ti3AlC2/Al2O3 nanocomposite powder was synthesized via mechanical alloying from TiO2, Al, and C as raw materials. Phase development and structural changes during ball milling were investigated by X-ray diffraction technique (XRD), field-emission gun scanning electron microscopy (FESEM) and transition electron microscopy (TEM). Results showed that TiAl, TiC and Al2O3 intermediate phases were formed after 20Â h milling of starting materials. With the increase of milling time to 40Â h, the desired Ti3AlC2/Al2O3 nanocomposite was achieved. It can be seen that Ti3AlC2 is not synthesized by a single reaction between TiO2, Al, and C and is occurred with a series of reactions between intermediate products (TiAl and TiC). TEM image of 40Â h milled powder confirmed that the synthesized Ti3AlC2/Al2O3 powder has nanosized particles in the range of 50Â nm.
Keywords
Related Topics
Physical Sciences and Engineering
Materials Science
Metals and Alloys
Authors
M. Zarezadeh Mehrizi, R. Beygi,