Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
7995017 | Journal of Alloys and Compounds | 2018 | 7 Pages |
Abstract
Fe80Ni20 was prepared by mechanical synthesis using a Fritsch Pulverisette Premium (P7) planetary ball mill at 400 RPM. The alloying process was monitored by measuring the magnetic properties of 14 subsamples taken at different milling times (1-2160Â min) as well as structural modifications using powder X-ray diffraction and high-resolution imaging. A macroscopically homogeneous body-centered cubic (bcc) alloy with crystallite sizes below 11Â nm and microstrain above 1.2% was reached after 960Â min (16Â h) of milling. The magnetic properties show three distinct stages: (1) the size reduction of the elementary powders, (2) alloying and (3) reduction in particle size of the final alloy.
Related Topics
Physical Sciences and Engineering
Materials Science
Metals and Alloys
Authors
Michael W.R. Volk, Michael R. Wack, Bernd J. Maier,