Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
8014823 | Materials Letters | 2018 | 14 Pages |
Abstract
A controlled growth of nano/micro rods with defined morphologies are of great interest due to its special and unique properties. Here we report ethylene glycol mediated facile and controlled synthesis of ultra-long (â¼100â¯Î¼m) perfect hexagon shaped microrods of silver molybdate by a cost effective method of hydrothermal. The exact conditions are optimized by varying the effective parameters. The synthesis involves the mixing of different concentration of silver nitrate solution (0.025, 0.075, 0.125â¯M) with ammonium molybdate in the presence of 10â¯ml of ethylene glycol and then post hydrothermal treatment at 150â¯Â°C for 12 hrs. Only 0.075â¯M conc. of silver nitrate results perfect hexagons whereas the lower and higher concentrations result the formation of distorted edge shaped and longer microrods of Ag6Mo10O33. The magnetic measurement shows the perfect diamagnetic behavior of these mircorods.
Related Topics
Physical Sciences and Engineering
Materials Science
Nanotechnology
Authors
Javier Enriquez Montenegro, Carolina Manquian Villalobos, Dinesh Pratap Singh,