Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
8038098 | Ultramicroscopy | 2015 | 12 Pages |
Abstract
High resolution, cross-correlation-based, electron backscatter diffraction (EBSD) measures the variation of elastic strains and lattice rotations from a reference state. Regions near grain boundaries are often of interest but overlap of patterns from the two grains could reduce accuracy of the cross-correlation analysis. To explore this concern, patterns from the interior of two grains have been mixed to simulate the interaction volume crossing a grain boundary so that the effect on the accuracy of the cross correlation results can be tested. It was found that the accuracy of HR-EBSD strain measurements performed in a FEG-SEM on zirconium remains good until the incident beam is less than 18Â nm from a grain boundary. A simulated microstructure was used to measure how often pattern overlap occurs at any given EBSD step size, and a simple relation was found linking the probability of overlap with step size.
Keywords
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Physical Sciences and Engineering
Materials Science
Nanotechnology
Authors
Vivian Tong, Jun Jiang, Angus J. Wilkinson, T. Ben Britton,