Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
8040474 | Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms | 2015 | 5 Pages |
Abstract
We present the general design features and preliminary performances of a new system for the simultaneous AMS-14C and IRMS δ13C and δ15N measurements on samples with masses in the μg range. The system consists of an elemental analyzer (EA), a gas splitting unit (GSU), a IRMS system, a gas handling interface (GHI) and a sputtering ion source capable of accepting gaseous samples. A detailed description of the system and of the control software supporting unattended operation are presented together with the first performance tests carried out by analyzing samples with masses ranging from 8 μgC to 2.4 mgC. The performances of the system were tested in term of stability of the ion beam extracted from the ion source, precision and accuracy of the results by comparing the measured isotopic ratios with those expected for reference materials.
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Authors
Eugenia Braione, Lucio Maruccio, Gianluca Quarta, Marisa D'Elia, Lucio Calcagnile,