Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
8155929 | Journal of Magnetism and Magnetic Materials | 2015 | 4 Pages |
Abstract
NiFe2O4/carbon nanofibers (NiFe2O4/CNFs) have been successfully synthesized by hydrotermal method using Venezuelan petroleum coke (petcoke) as carbon source and NiFe2O4 as catalyst. The morphology, structural and magnetic properties of nanocomposite products were characterized by X-ray diffraction (XRD), high-resolution transmission electron microscopy (HR-TEM), vibrating sample magnetometry (VSM) and electron paramagnetic resonance (EPR). XRD analysis revealed a cubic spinel structure and ferrite phase with high crystallinity. HR-TEM reveals the presence of CNFs with diameters of 4±2 nm. At room temperature, NiFe2O4/CNFs show superparamagnetic behavior with a maximum magnetization of 15.35 emu/g. Our findings indicate that Venezuelan petroleum coke is suitable industrial carbon source for the growth of magnetic CNFs.
Related Topics
Physical Sciences and Engineering
Physics and Astronomy
Condensed Matter Physics
Authors
Sarah Briceño, Pedro Silva, Wilmer Molina, Werner Brämer-Escamilla, Olgi Alcalá, Edgard Cañizales,