| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 829260 | Materials & Design (1980-2015) | 2014 | 7 Pages |
•PN + LQ treatment results in thicker layer depth than single PN or LQ treatment.•The increase of layer depth is caused by the eutectoid point reduction due to introduction of N.•LQ treatment cause the brittle phase decomposed and the hardness redistributed of PN specimen.•PN + LQ specimen shows better wear resistance than the PN counterpart.
30CrMnSiA steel has been commonly used in many industrial applications owing to its excellent mechanical properties. However, raw 30CrMnSiA steel cannot meet the requirements of practical application, such as high surface hardness and superior wear resistance. In practice, plasma nitriding (PN) is usually conducted to strengthen the surface properties of this steel. However conventional plasma nitriding (PN) technique is always hindered by diffusion kinetics. Alternatively, the process of laser quenching (LQ) has been utilized as a unique rapid method for tailoring the surface microstructure and chemical composition to improving the mechanical properties of steels. In the present study, a laser quenching technique (LQ) is utilized as subsequent procedure of typical plasma nitriding treatment process (PN) to improve the surface properties of 30CrMnSiA steel. The microstructure and properties of such layer are compared with those obtained by PN or LQ treatment. OM, XRD, SEM and EDS analysis are conducted for microstructure observation, phase identification, and estimating the nitrogen concentration, respectively. Microhardness tester and pin-on-disc tribometer are used to investigate the mechanical properties of the modified layers. Laser quenching of plasma nitrided (PN + LQ) 30CrMnSiA steel results in great increase in the thickness and hardness of the modified layer comparing with the PN and LQ treatment due to the reduction of eutectoid point caused by introduction of nitrogen. The mechanism is also discussed systematically based on the phase diagram in the paper. Moreover, the layer treated by PN + LQ process exhibits better wear resistance than the PN treated specimen. This is attributed to the formation of retained austenite and Fe3O4 according to the XRD analysis, which is beneficial to the improvement of impact toughness and the lubrication action during sliding.
