Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
9594178 | Solid State Nuclear Magnetic Resonance | 2005 | 5 Pages |
Abstract
We show that it is possible to efficiently transfer magnetization from 31P to 29Si, using variable amplitude CP MAS experiment. This experiment is demonstrated by using Si5O(PO4)6, the synthesis protocol of which is described. From the obtained results, we show that the experiment allows the spectral edition of 29Si spectra from 31Pâ29Si CP, enabling the studies of derivatives involving Si-O-P linkages, such as phosphosilicate glasses, microporous silicoaluminophosphates (SAPO) and bioactive phosphosilicates.
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Physical and Theoretical Chemistry
Authors
Clarisse Lejeune, Cristina Coelho, Laure Bonhomme-Coury, Thierry Azaïs, Jocelyne Maquet, Christian Bonhomme,