Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
9594181 | Solid State Nuclear Magnetic Resonance | 2005 | 5 Pages |
Abstract
We demonstrate that the finite pulse RFDR sequence (J. Chem. Phys. 114 (2001) 8473) can be used effectively for 31P double-quantum NMR spectroscopy at a spinning frequency of 10Â kHz. The 31P NMR data measured for hydroxyapatite and octacalcium phosphate show that sizable double-quantum excitation efficiency can be obtained with the ratio of the recoupling field to spinning frequency set equal to 1.67.
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Physical Sciences and Engineering
Chemistry
Physical and Theoretical Chemistry
Authors
Yao-Hung Tseng, Yun Mou, Chung-Yuan Mou, Jerry C.C. Chan,