Article ID Journal Published Year Pages File Type
9594181 Solid State Nuclear Magnetic Resonance 2005 5 Pages PDF
Abstract
We demonstrate that the finite pulse RFDR sequence (J. Chem. Phys. 114 (2001) 8473) can be used effectively for 31P double-quantum NMR spectroscopy at a spinning frequency of 10 kHz. The 31P NMR data measured for hydroxyapatite and octacalcium phosphate show that sizable double-quantum excitation efficiency can be obtained with the ratio of the recoupling field to spinning frequency set equal to 1.67.
Related Topics
Physical Sciences and Engineering Chemistry Physical and Theoretical Chemistry
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