Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1170675 | Analytica Chimica Acta | 2007 | 8 Pages |
Nineteen different dietary supplements, ordered through the internet and intercepted by the Belgian pharmaceutical inspection at the post office, were analyzed by means of liquid chromatography–tandem mass spectrometry (LC–MS/MS) for the presence of anabolic steroids. After a methanolic extraction the samples were screened for the presence of 49 compounds. This resulted in almost 60% of the samples being suspected of containing one of these 49 anabolic compounds and being subjected to a confirmatory product ion scan. In all of these suspected samples we were able to confirm at least one anabolic steroid with concentrations between 0.01 and 2.5 mg unit−1 (unit: one capsule or tablet or for liquids: the prescribed dose). The anabolic steroids that was mostly encountered was testosterone (50%) followed by β-boldenone (25%). These results once more confirm the dubious reputation of over-the-counter dietary supplements.