| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 1282466 | International Journal of Hydrogen Energy | 2011 | 18 Pages |
The API 5L X70 and X52 pipeline steel weld fracture toughness parameters are measured in a hydrogen environment and compared to the ones in air. The hydrogen environment is created by in situ hydrogen charging, using as an electrolyte a simulated soil solution, with three current densities, namely 1, 5 and 10 mA/cm2. A specially designed electrolytic cell mounted onto a three-point bending arrangement is used and hydrogen charging is performed during the monotonic loading of the specimens. Ductility is measured in terms of the J0 integral. In all cases a slight change in toughness was measured in terms of KQ. Reduction of ductility in the base metal is observed, which increases with increasing current density. A more complex phenomenon is observed in the heat affected zone metal, where a small reduction in ductility is observed for the two current densities (1 and 5 mA/cm2) and a larger reduction for the third case (10 mA/cm2). Regarding microstructure of tested X70 and X52 base and HAZ metal, it is observed that the hydrogen degradation effect is enhanced in banded ferrite–pearlite formations. The aforementioned procedure is used for calculating the fracture toughness parameters of a through-thickness pipeline crack.
► Pipeline steel welds fracture toughness is examined against hydrogen environment. ► In situ hydrogen charging is used using various current densities. ► Large reduction of J0 is observed for the base metal and small reduction for the HAZ. ► Banded ferrite–pearlite microstructure is detrimental for hydrogen reduction of J0. ► Damage type is hydrogen embrittlement.
