Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1405434 | Journal of Molecular Structure | 2013 | 5 Pages |
Abstract
A new solvatomorph of gallic acid was generated using chiral additive technique and characterized by single crystal and powder X-ray diffraction, C-13 NMR, IR spectroscopic techniques and thermal analysis. The supramolecular channels formed by hexameric motifs of gallic acid and solvent molecules contain highly disordered solvent molecules with fractional occupancies.
► The crystal structure of fifth solvatomorph of gallic acid. ► Crystal form generated by chiral additive. ► Supramolecular channel structure with highly disordered solvents. ► Phase transition studies show the uniqueness of anhydrous form. ► “Hydration synthons” formed by water molecules analyzed.
Keywords
Related Topics
Physical Sciences and Engineering
Chemistry
Organic Chemistry
Authors
Sajesh P. Thomas, Ramanpreet Kaur, Jassjot Kaur, Ravish Sankolli, Susanta K. Nayak, Tayur N. Guru Row,