Article ID Journal Published Year Pages File Type
1405434 Journal of Molecular Structure 2013 5 Pages PDF
Abstract

A new solvatomorph of gallic acid was generated using chiral additive technique and characterized by single crystal and powder X-ray diffraction, C-13 NMR, IR spectroscopic techniques and thermal analysis. The supramolecular channels formed by hexameric motifs of gallic acid and solvent molecules contain highly disordered solvent molecules with fractional occupancies.

► The crystal structure of fifth solvatomorph of gallic acid. ► Crystal form generated by chiral additive. ► Supramolecular channel structure with highly disordered solvents. ► Phase transition studies show the uniqueness of anhydrous form. ► “Hydration synthons” formed by water molecules analyzed.

Related Topics
Physical Sciences and Engineering Chemistry Organic Chemistry
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