Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1480688 | Journal of Non-Crystalline Solids | 2015 | 9 Pages |
Abstract
A three-step preparation procedure of the silicon oxynitrocarbide (SiONC) glass was developed, for the purpose of the production of SiONC composites with inorganic fibres. At first, a stable, storable viscous liquid precursor resin (suitable for fibre impregnation) was synthesized via hydrosilylation. The liquid resin was subsequently cured via radical polymerization in the second step, and finally, the solid precursor was pyrolysed to SiONC. Two SiONC glasses, with higher and with lower oxygen content, were prepared and characterized. Weight losses during processing, the compactness (electron microscopy) of the prepared glasses, their elemental composition (energy-dispersive X-ray spectroscopy) and chemical microstructure (nuclear magnetic resonance), as well as their mechanical properties (indentation moduli and compression strength) were investigated. Finally, the three-step SiONC synthesis was successfully employed to prepare a SiONC/Nextel 720 fibre composite, which displayed very good mechanical properties.
Related Topics
Physical Sciences and Engineering
Materials Science
Ceramics and Composites
Authors
Adam Strachota, Martin Äerný, ZdenÄk Chlup, Miroslav Å louf, JiÅà Brus, Josef PleÅ¡til, ZbynÄk Sucharda, Martina Havelcová, Martina Halasová,