Article ID Journal Published Year Pages File Type
1569397 Journal of Nuclear Materials 2007 5 Pages PDF
Abstract

The morphological and microstructural properties of powder particles were examined systematically to optimize the milling time for producing high-chromium oxide dispersion strengthened (ODS) ferritic steels. The XRD and SEM results showed that peak broadening in the XRD patterns occurred due to a decrease in the grain size and the particle diameter of the powder during mechanical milling. The particle size distribution range decreased first with increasing the milling time up to 12 h and then clearly increased thereafter. After 12 h milling, the particles were nearly spherical with nearly uniform mean size of 5.9 μm. SEM–EDS analysis of the particle surface showed all distributed homogeneously.

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Physical Sciences and Engineering Energy Nuclear Energy and Engineering
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