Article ID Journal Published Year Pages File Type
1569877 Journal of Nuclear Materials 2006 7 Pages PDF
Abstract

An atom probe tomography microstructural characterization has been performed on an A533B pressure vessel steel (JRQ) after irradiation to a fluence of 5 × 1023 n m−2 (E > 1 MeV) and a subsequent annealing treatment of 168 h at 460 °C and also through two cycles of neutron irradiation (0.85 × 1023 n m−2 (E > 1 MeV)) and annealing (168 h at 460 °C). The alloy that was neutron irradiated to a fluence of 5 × 1023 n m−2 exhibited a high number density of Cu-enriched precipitates and a shift in the ductile-to-brittle transformation temperature of ΔT41J = 96 °C. Annealing for 168 h at 460 °C coarsened these Cu-enriched precipitates and recovered the embrittlement. The material that was re-irradiated to a total fluence 1.7 × 1023 n m−2 also exhibited a high number density of Cu-enriched precipitates and a ΔT41J shift of 56 °C. Annealing the re-irradiated material for 168 h at 460 °C coarsened these precipitates and recovered the embrittlement.

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Physical Sciences and Engineering Energy Nuclear Energy and Engineering
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