| Article ID | Journal | Published Year | Pages | File Type |
|---|---|---|---|---|
| 2029124 | Steroids | 2016 | 4 Pages |
Abstract
•Glucuronide N-histaminyl amide preparation.•Immunoanalytical kit component.•Improved glucuronide synthesis.•5α-Androstane-3α,17β-diol conjugate.
Simple method of preparation of 5α-androstane-3α,17β-diol 17-O-glucuronide N-histaminyl amide was developed for the construction of immunoanalytical kit. Improved method of glucuronide derivative synthesis was used, followed by hydroxybenzotriazole–dicyclohexylcarbodiimide coupling with histamine.
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Authors
Petr Vinš, Ivan Černý, Petra Mikšátková, Pavel Drašar,