Article ID Journal Published Year Pages File Type
596010 Colloids and Surfaces A: Physicochemical and Engineering Aspects 2009 6 Pages PDF
Abstract
In this paper, monodisperse Fe3O4 nanoparticles with single crystalline structure were synthesized via a facile environment-friendly method. And the size of the nanoparticles ranges from 10 nm to 15 nm. As-synthesized Fe3O4 were characterized by X-ray diffraction instrument (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared (FT-IR) spectrometer and field emission transmission electron microscope (FE-TEM). The effect of tartaric acid (TA) amount on products was investigated by XRD and TEM. The results indicated that TA could commendably modulate the crystalline phase, morphology and size of nanometer Fe3O4. A possible generated mechanism of Fe3O4 crystals was proposed in virtue of UV-vis absorption spectra. Besides, the magnetic properties of as-synthesized Fe3O4 were detected.
Related Topics
Physical Sciences and Engineering Chemical Engineering Colloid and Surface Chemistry
Authors
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