Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
598321 | Colloids and Surfaces A: Physicochemical and Engineering Aspects | 2006 | 4 Pages |
Abstract
A series of commercial fibers (carbowax–divinylbenzene, carboxen–polydimethylsiloxane, polydimethylsiloxe–divinylbenzene, divinylbenzene/carboxen polydimethylsiloxane and polyacrylate were evaluated for pre-concentration of acetone in cyclohexane by solid phase microextraction (SPME). Fibers were evaluated in terms of exposure time, extraction temperature and stirring. Best results were observed for divinylbenzene/carboxen polydimethylsiloxane with extraction temperature of 40 °C and 15 min of extraction time. The quantification range was situated at ppb level. Evaluation of the method in an industrial polymerization plant effluent was shown to be efficient.
Related Topics
Physical Sciences and Engineering
Chemical Engineering
Colloid and Surface Chemistry
Authors
Maria Angélica C. Gollmann, Maria do Carmo R. Peralba, Tânia M. Pizzolato, João Henrique Zimnoch dos Santos, Marcello José Rodrigues Cavalcanti,