Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1305060 | Inorganic Chemistry Communications | 2006 | 4 Pages |
A series of novel N-meta-ferrocenyl benzoyl dipeptide esters (2–5) have been prepared by coupling meta-ferrocenyl benzoic acid (1) to the dipeptide ethyl esters using the conventional 1,3-dicyclohexylcarbodiimide (DCC), 1-hydroxybenzotriazole (HOBt) protocol. The dipeptides employed were GlyGly(OEt) (2), GlyAla(OEt) (3), GlyLeu(OEt) (4) and GlyPhe(OEt) (5). The compounds were fully characterized by a range of NMR spectroscopic techniques and by mass spectrometry (MALDI-MS, ESI-MS).
Graphical abstractN-meta-ferrocenyl benzoyl dipeptide ethyl esters (2–5) have been prepared by coupling meta-ferrocenyl benzoic acid (1) to the dipeptide ethyl esters using the conventional 1,3-dicyclohexylcarbodiimide (DCC), 1-hydroxybenzotriazole (HOBt) protocol. The dipeptides employed were GlyGly(OEt) (2), GlyAla(OEt) (3), GlyLeu(OEt) (4) and GlyPhe(OEt) (5). The compounds were structurally characterized by a combination of NMR spectroscopic techniques and mass spectrometry (MALDI-MS, ESI-MS).Figure optionsDownload full-size imageDownload as PowerPoint slide