Article ID Journal Published Year Pages File Type
620467 Chemical Engineering Research and Design 2015 12 Pages PDF
Abstract

•A mid-course correction strategy based self-tuning final product quality control of batch processes is presented.•KPLS model is used to deal with the nonlinear problem.•The unknown future trajectories are estimated using multi-PCA models.•The soft constraint on the score magnitude is used to constrain the solution in the kernel latent variable space of KPLS model.•Heuristic rule is used for weighting factor to balance the control objective and score magnitude.

A mid-course correction (MCC) strategy based self-tuning final product quality control of batch processes is presented. The method employs KPLS model developed using batch-wise unfolding data set to capture the relationship between the process variables and final quality. The estimators for the future unknown trajectories are accomplished using statistical latent variable missing data imputation method based on multi-PCA models. Then the optimal control problem is formulated such that the solution is constrained to lie in the kernel latent variable space of the model defined by historical batch data set, and heuristic rule is used for weighting factor to balance the control objective and score magnitude. Finally, SQP is implemented to solve the constraint optimization problem. Application to a simulated cobalt oxalate synthesis process demonstrates that the proposed modeling and quality control strategy can improve process performance.

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Physical Sciences and Engineering Chemical Engineering Filtration and Separation
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