Article ID | Journal | Published Year | Pages | File Type |
---|---|---|---|---|
1254760 | Chinese Chemical Letters | 2011 | 4 Pages |
Abstract
A combination of photochlorination of p-xylene and succedent Friedel–Crafts alkylation polymerization was firstly used in the preparation of the hypercrosslinked adsorptive resin. The data of GC–MS and GC showed that a series of chlorizates were produced when p-xylene was photochlorinated. Hypercrosslinked resins could be synthesized by copolymerization, self-polymerization of chlorizates or post crosslinking reaction. The chemical structure and micromorphology of the porous resins were characterized by BET, FT-IR, SEM and elementary analysis (EA). The results showed that the novel adsorptive resins possess high BET surface near to 1038 m2/g and large pore volumes range from 0.5 to 1.2 cm3/g.
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Authors
Ling Ling Bai, Yong Hao Zhou, Xiu Li Wang, Si Guo Yuan, Xian Li Wu,